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Thermal Stability of Novel Multilayer Lanthanum Zirconate Based Thermal Barrier Coatings

机译:新型多层锆钛酸镧基热障涂层的热稳定性

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摘要

This chapter discusses the thermal stability of SCL and DCL porous La2Zr2O7 coats by depositing three types of SCL and DCL La2Zr2O7 and 8YSZ structures in an experiment. Heat treatment, cyclic furnace cycle test and jet engine thermal shock test were conducted for the thermal barrier coatings (TBC) samples. The heating and cooling cycles were repeated until cracks or spallation were spotted on the TBC surface. Both the front and back surface temperatures were measured using pyrometer. The delamination is caused by the thermal residual stress induced by CTE difference between La2Zr2O7 and 8YSZ. All the La2Zr2O7 coats were delaminated in the furnace cycle test in less than 20 cycles. This is because residual thermal stresses accumulated during thermal cycling. Microstructure images of heat treated samples were taken using a scanning electron microscope.
机译:本章通过在实验中沉积三种类型的SCL和DCL La2Zr2O7和8YSZ结构,讨论了SCL和DCL多孔La2Zr2O7涂层的热稳定性。对隔热涂层(TBC)样品进行了热处理,循环炉循环试验和喷气发动机热冲击试验。重复加热和冷却循环,直到在TBC表面上发现裂纹或剥落。使用高温计测量正面和背面温度。分层是由La2Zr2O7和8YSZ之间的CTE差异引起的热残余应力引起的。所有的La2Zr2O7涂层在炉子循环测试中均在不到20个循环中分层。这是因为在热循环期间累积了残余热应力。使用扫描电子显微镜拍摄热处理样品的显微图像。

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